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Main menu for Browse IS/STAG
Course info
ACH / UAOS
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Course description
Department/Unit / Abbreviation
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ACH
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UAOS
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Academic Year
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2024/2025
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Academic Year
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2024/2025
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Title
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Analysis of Organic Compounds
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Form of course completion
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Exam
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Form of course completion
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Exam
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Accredited / Credits
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Yes,
7
Cred.
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Type of completion
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Combined
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Type of completion
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Combined
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Time requirements
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Lecture
4
[Hours/Week]
Seminar
2
[Hours/Week]
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Course credit prior to examination
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Yes
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Course credit prior to examination
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Yes
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Automatic acceptance of credit before examination
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No
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Included in study average
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YES
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Language of instruction
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Czech, English
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Occ/max
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Automatic acceptance of credit before examination
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No
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Summer semester
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0 / -
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0 / -
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0 / -
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Included in study average
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YES
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Winter semester
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0 / -
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0 / -
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0 / -
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Repeated registration
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NO
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Repeated registration
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NO
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Timetable
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Yes
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Semester taught
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Winter semester
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Semester taught
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Winter semester
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Minimum (B + C) students
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not determined
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Optional course |
Yes
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Optional course
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Yes
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Language of instruction
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Czech, English
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Internship duration
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0
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No. of hours of on-premise lessons |
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Evaluation scale |
A|B|C|D|E|F |
Periodicity |
každý rok
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Evaluation scale for credit before examination |
S|N |
Periodicita upřesnění |
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Fundamental theoretical course |
No
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Fundamental course |
No
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Fundamental theoretical course |
No
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Evaluation scale |
A|B|C|D|E|F |
Evaluation scale for credit before examination |
S|N |
Substituted course
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None
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Preclusive courses
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N/A
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Prerequisite courses
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N/A
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Informally recommended courses
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N/A
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Courses depending on this Course
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N/A
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Histogram of students' grades over the years:
Graphic PNG
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XLS
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Course objectives:
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The aim is to familiarize with facilities of analysis of organic compounds.
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Requirements on student
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Requirement: active attendance in seminars (75 %), written seminar work (seminar), oral exam (lecture)
Requirement: active attendance in seminars (75 %), examination paper (seminar), oral exam (lecture)
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Content
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Analysis of organic compounds Sample characterization, sampling, preparatory operations, drying, purity characterization, appearance examination. Physico-chemical constants (melting point, boiling point, density, refractive index, specific rotation, solubility, partition coefficient) and their relations to the chemical structure. Instrumental methods of chemical analysis - spectrometric methods (UV-Vis spectrometry, infrared spectrometry, nuclear magnetic resonance, mass spectrometry, optical rotary dispersion), electrochemical methods (voltammetry, coulometry) separation methods (extraction, gas chromatography, liquid chromatography, electrophoresis, isotachophoresis). Organic elemental analysis. Principles and techniques of proofs, identification and determination of organic compounds and their mixtures. General principles of classical methods of organic analysis. Titrations in non-aqueous media. Proof and determination of functional groups - hydrocarbons, hydroxycompounds, carbonylcompounds, carboxylic acids and their functional derivatives, nitrogen containing compounds, sulphur containing compounds, halogen containing compounds, selected polyfunctional derivatives. Instrumental methods and their application for particular groups of organic compounds. Analytical derivatization.
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Activities
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Fields of study
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Guarantors and lecturers
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Literature
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-
Recommended:
Pavia D.L., lampman G.M., Hriz G.S., Engel R.G. A Small Scale Approach to organic Laboratory Techniques. belmont, 2011.
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Recommended:
Kellner R., Mermet J.-M., Otto M., Valcárcel M., Widmer, H. M. Analytical Chemistry. A Modern Approach to Analytical Science. Wiley-VCH, Weinheim, 2004.
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Recommended:
Christian G.D., Dasqupta P.K., Schug K.A. Analytical chemistry 7th. ed.. Wiley Hoboken, 2014.
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Recommended:
Štulík K., Ševčík J., Pacáková V., Jelínek I., Coufal P., Bosáková Z. Analytické separační metody. Karolinum Praha, 2004.
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Recommended:
Stránský Z. a kol. Analýza organických sloučenin. RUP Olomouc, 1981.
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Recommended:
Jandera P. Atomová a molekulová spektroskopie se zaměřením na stopovou analýzu kontaminantů, díl B. Univerzita Pardubice, 1999.
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Recommended:
Večeřa M., Gasparič J. Detection and identification of organic compounds. Plenum Press, 1971.
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Recommended:
Večeřa M., Gasparič J. Důkaz a identifikace organických látek. Praha, 1963.
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Recommended:
I. Wilson, C. Poole, M. Cooke. Encyclopedia of separation science. Academic Press, San Diego, London, Boston, New York, Sydney, Tokyo, Toronto, 2000.
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Recommended:
maloň P., Podlaha J., Ubik K. Fyzikálně chemické metody 1-3. AVČR, 2000.
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Recommended:
Harvey D. Modern Analytical Chemistry. McGraw-Hill, New York, 2000.
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Recommended:
Churáček J. a kol. Nové trendy v teorii a instrumentaci vybraných analytických metod. Praha, 1993.
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Recommended:
Jureček M. Organická analysa I a II. Nakladatelství ČSAV Praha, 1957.
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Recommended:
Jureček M.. Organická analýza. Praha, 1950.
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Recommended:
McMurry J. Organická chemie. Praha, 2007. ISBN 978-80-7080-637-1.
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Recommended:
Beyerman K.. Organická stopová analýza. SNTL Praha, 1987.
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Recommended:
Veibel S. Praktická příručka organické analýzy. Praha, 1963.
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Recommended:
Němcová I., Engst P., Jelínek J., Sejbal J. Spektrometrické analytické metody II. Karolinum, 1998.
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Recommended:
J.R. Mohrig, Ch.N. Hammond, P.F. Schatz. Techniques in Organic Chemistry. W.H. Freeman and Company, New York, 2010.
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Recommended:
Shriner R. a kol. The systematic identification of organic compounds. Wiley Hoboken, 2004.
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On-line library catalogues
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Time requirements
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All forms of study
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Activities
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Time requirements for activity [h]
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Attendace
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78
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Preparation for the Exam
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50
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Preparation for the Course Credit
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30
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Homework for Teaching
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52
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Total
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210
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Prerequisites - other information about course preconditions |
The knowledge of basics of organic and analytical chemistry is recommended. |
Competences acquired |
Associate information, interpret experimental data, solve problems, interpret the structure of substances on the basis of spectral data and chemical reactivity |
Teaching methods |
- Lecture
- Dialogic Lecture (Discussion, Dialog, Brainstorming)
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Assessment methods |
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