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Lecturer(s)
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Jirovský David, doc. RNDr. Ph.D.
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Course content
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Solid electrodes, chemically modified electrodes and microelectrodes, electrochemical sensors. Methods for the study of electrode reactions: cyclic voltammetry, pulse and AC voltammetry, spectroelectrochemistry, scanning electrochemical microscopy, electrochemical quartz crystal microbalance. Electrochemical flow-analysis, electrochemical detection in HPLC, amperometric detectors, coulometric detectors, multi-electrode array detectors, applications of multichannel electrochemical detection for analysis of bioactive compounds. Electrochemistry on-line with mass spectrometry (EC MS) - perspectives and application in study of redox biochemical systems.
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Learning activities and teaching methods
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Dialogic Lecture (Discussion, Dialog, Brainstorming)
- Attendace
- 20 hours per semester
- Preparation for the Exam
- 80 hours per semester
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Learning outcomes
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Solid electrodes, chemically modified electrodes and microelectrodes, electrochemical sensors. Methods for the study of electrode reactions: cyclic voltammetry, pulse and AC voltammetry, spectroelectrochemistry, scanning electrochemical microscopy, electrochemical quartz crystal microbalance. Electrochemical flow-analysis, electrochemical detection in HPLC, amperometric detectors, coulometric detectors, multi-electrode array detectors, applications of multichannel electrochemical detection for analysis of bioactive compounds. Electrochemistry on-line with mass spectrometry (EC MS) - perspectives and application in study of redox biochemical systems.
Explain up to date novelties in electroanalytical methods, compare methods, explain results.
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Prerequisites
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Successfully graduation master's programme Analytical chemistry
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Assessment methods and criteria
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Student performance
To become acquainted with the subject matter according to guarantor or teacher recommendations and prove capability to explain and discuss given topic.
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Recommended literature
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Acworth, I.N., Naoi, M., Parvez, H., Parvez, S. (Eds). (1997). Coulometric electrode array detectors for HPLC. VSP BV, Utrecht.
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Alkire, R. C., Kolb, D. M., Lipkowski, J., Ross, P. (2009). Chemically Modified Electrodes. Wiley-VCH, Weinheim.
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Bard, A. J., Faulkner, L. R. (2001). Electrochemical Methods. Wiley, New York.
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Cooper, J. M., Cass, A. E. G. (Eds). (2004). Biosensors. Oxford University Press.
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Flanagan, R. J., Perrett, D., Whelpton, R. (2005). Electrochemical Detection in HPLC: Analysis of Drugs and Poisons. RSC, Cambridge.
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Scholz F. (2002). Electroanalytical methods: Guide to Experiments and Applications. Springer, Berlín.
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Trojanowicz, M. (2000). Flow injection analysis: instrumentation and applications. World Scientific, Singapore.
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Wang, J. (2006). Analytical electrochemistry. Wiley-VCH, NY.
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Wang, J. (1988). Electroanalytical Techniques in clinical chemistry and laboratory medicine. VCH Publishers, Weinheim.
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