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Lecturer(s)
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Kupka Vojtěch, Ing. Ph.D.
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Kvítek Libor, prof. RNDr. CSc.
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Berka Karel, prof. RNDr. Ph.D.
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Course content
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The lectures include thermography, magnetochemistry, crystalographic methods, microscopic methods, Mössbauer spectroscopy, methods of studying the particle size distribution and viscosity-elastic properties. 1. Optical microscopy. 2. Electron microscopy. 3. AFM-atomic force microscopy. 4. Crystals, types of crystal structures, stereochemistry of selected compounds. 5. X-ray analysis-monocrystal and powder methods. 6. Thermic analysis methods. 7. Magnetochemistry-theoretical introduction, key terminology and variables-paramagnetism, diamagnetism and their chemical interpretation-magnetic susceptibility measurements. 8. Mössbauer spectroscopy. 9. Studyof the solid surface energy. 10. Methods of studying the particle size distribution. 11. Viscosity-elastic properties of substances. 12. Study trip-instrumentation.
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Learning activities and teaching methods
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Monologic Lecture(Interpretation, Training)
- Preparation for the Exam
- 90 hours per semester
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Learning outcomes
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This lecture is focused on physico-chemical methods used in study of solid substances.
ability to associate information, explain main principles of the methods for the investigation of solid state
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Prerequisites
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unspecified
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Assessment methods and criteria
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Written exam
Successful fulfilment of the credit test in 60%
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Recommended literature
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Györyová, K., Bálek, V. (1992). Termická analýza. skriptum UJPŠ Košice.
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Kubínek R. (1986). Experimentální metody biofyziky-Rastrovací elektronová mikroskopie.. Učební text UP.
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1. Jiří Fišer:. (1980). Úvod do molekulové symetrie (Aplikace teorie grup v chemii) : Mikroskopie skenující sondou. Vydavatelství UP 2002 (v tisku) 12. http://www.upol.cz/resources/exfyz/bf/expmet1.htm . SNTL Praha.
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10. L. Reimer. (1998). Scanning Electron Microscopy - Physics of Image Formation and Microanalysis.. Springer.
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2. František Březina a kol.:. (1988). Stereochemie a některé fyzikálně-chemické metody studia anorganických látek.. Scrpt. UP Olomouc, II.vyd.
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3. Václav Prosser. (1989). Experimentální metody biofyziky,. : Academia Praha.
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4. E.A.Boudroux, L.N.Mulay:. (1976). Theory and applications of molecular paramagnetism,. Wiley&Sons N.Y.
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5. F.E.Mabbs, D.J.Machin:. (1973). Magnetism and Transition Metal Complexes. Chapman and Hall, London.
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6. J. Rosický:. (1989). Termická analýza. Praha.
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8. Ed. C. Giacivazzo. (1992). Fundamentals of Crystallography,. Oxford University Press, IUCr, ().
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