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Lecturer(s)
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Štarha Pavel, doc. Mgr. Ph.D.
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Drahoš Bohuslav, doc. RNDr. Ph.D.
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Course content
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" Introduction, safety rules " Elemental analysis, conductivity measurements " Nuclear magnetic resonance (NMR) " Electron spectroscopy, emission spectroscopy, X-ray fluorescence (XRF) " Infrared and Raman spectroscopy " High-performance liquid chromatography and mass spectrometry (HPLC-MS) " Magnetochemistry " Single-crystal and powder X-ray diffraction analysis " Cyclic voltammetry " Atomic absorption spectrometry " Excursion (Mössbauer spectroscopy) " Colloquium
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Learning activities and teaching methods
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Laboratory Work
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Learning outcomes
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The practice Methods for study of inorganic compounds is designed for advanced inorganic chemistry students and their instrumental skill for practical applications.
Apply the theoretical knowledge for concrete physical-chemical measurements using selected methods.
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Prerequisites
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Basic theoretical knowledge of each method.
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Assessment methods and criteria
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Student performance
The student has to attend all exercises. Minimal success in the written tests has to be at least 70%. Correct laboratory protocols from all exercises have to be given.
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Recommended literature
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D. W. H. Rankin, N. W. Mitzel, C. A. Morrison. (2013). Structural methods in molecular inorganic chemistry. Wiley, UK.
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J. Garaj a kol. (1977). Fyzikálné a fyzikálne-chemické analytické metódy. Alfa, Bratislava.
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Kameníček, J. (1992). Cvičení z fyzikálně chemických metod studia látek. UP, Olomouc.
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V. Kalous a kolektiv. (1987). Metody chemického výzkumu. SNTL/Alfa, Praha.
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