Course: Crystal Structure and X-ray Diffraction

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Course title Crystal Structure and X-ray Diffraction
Course code AFC/KSRD
Organizational form of instruction Lecture
Level of course Master
Year of study not specified
Semester Winter
Number of ECTS credits 3
Language of instruction Czech
Status of course Compulsory, Compulsory-optional
Form of instruction Face-to-face
Work placements This is not an internship
Recommended optional programme components None
Lecturer(s)
  • Nemec Ivan, Ing. Ph.D.
Course content
- introduction - history, basic terms (definition of crystal, lattice types, Miller's indexes, crystallographic systems, minimal symmetry rules, reciprocal lattice) - point symmetry, stereographic projection - group theory, crystallographic group of symmetry, symbols - matrix representation of symmetry operations - space group of symmetry; symbols, graphical illustration - crystallochemistry, crystallization processes, types of structure defects - crystal structure and chemical bond - X-ray; principle, formation, forms, properties, registration, units - interaction with matter - ESCA, fluorescence, Auger electrons - diffraction of X-rays; Laue and Bragg equations; structural factor F(hkl) - X-ray diffraction methods, classification based on Ewald's scheme, Laue, Debye Scherrer, powder methods - powder diffractometers, indexation of powder patterns records, focusing methods, practical applications of powder methods - single crystal techniques; Weissenberg and precession method, types of diffractometers, complete X-ray analysis of crystal compounds

Learning activities and teaching methods
Lecture
Learning outcomes
The lecture Crystal structure and X-ray diffraction is designed for advanced inorganic chemistry students and it covers crystallography and X-ray diffraction methods.
recall basic terms of crystallography. X-ray and its application to structure of compounds by X-ray diffraction methods.
Prerequisites
unspecified

Assessment methods and criteria
Oral exam

Participation of all lectures is recommended.
Recommended literature
  • B. Kratochvíl. (1988). Základy fyziky a chemie pevných látek. VŠCHT, Praha.
  • F. Březina a kolektiv. (1994). Stereochemie a některé fyzikálně chemické metody studia anorganických látek. UP, Olomouc.
  • J. Chojnacki. (1979). Základy chemické a fyzikální krystalografie. Academia, Praha.
  • J. Loub. (1982). Krystalová symetrie a rentgenová difrakce. UK, Praha.
  • Kraus, I. (1995). Úvod do strukturní rentgenografie. Academia, Praha.
  • Z. Žák. (1982). Rentgenová difrakce a studium struktury látek. MU, Brno.


Study plans that include the course
Faculty Study plan (Version) Category of Branch/Specialization Recommended year of study Recommended semester
Faculty: Faculty of Science Study plan (Version): Nanomaterial Chemistry (2021) Category: Chemistry courses 1 Recommended year of study:1, Recommended semester: Winter
Faculty: Faculty of Science Study plan (Version): Inorganic and Bioinorganic Chemistry - specialization in Bioinorganic Chemistry (2021) Category: Chemistry courses 1 Recommended year of study:1, Recommended semester: Winter
Faculty: Faculty of Science Study plan (Version): Inorganic and Bioinorganic Chemistry - specialization in Inorganic Materials (2021) Category: Chemistry courses 1 Recommended year of study:1, Recommended semester: Winter
Faculty: Faculty of Science Study plan (Version): Nanomaterial Chemistry (2021) Category: Chemistry courses 1 Recommended year of study:1, Recommended semester: Winter