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Lecturer(s)
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Bednář Petr, doc. RNDr. Ph.D.
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Course content
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Normative activities, standards of quality, standard analytical procedures. Hierarchy of norms - ISO, ČSN. Good laboratory practice (GLP). Accreditation of procedures and laboratories. Inter-laboratory control, circular tests, international cooperation. Correct sampling, sampel treatment, strategy of analytical procedure choice (isolation, suppression of matrix effects, preconcentration, choice of proper of measurement and detection technique). Food analysis. Macro and micro components. Inorganic components of food, determination of macro nad microelements. Detemination of water and carbon dioxide. Determination of proteins, linked and free aminoacids, other nitrogen components. Determination of lipids, their separation, control of ageing process and nutritive quality. Isolation, proof and determination of mono, oligo and polysaccharides. Analysis of antioxidants and conservation agents. Isolation, identification and determination of undesirable components in food - pesticide residues, toxins. Forensic analysis. Control of input of toxic compounds into body and their metabolism. Inorganic toxic compounds and their determination. White damp (CO) poisoning, chronic poisoning by some cations. Determination of alcohol and other volatile organic toxicants in body. Determination of extractable poisons and drugs. Classical and modern extraction procedures. Chromatography and electrophoresis in forensic analysis. Analysis of macromolecules and polymers. Technical evaluation and identification of polymers. Analytical reactions. Physicochemical constants suitable for identification, evaluation of crystallinity and microstructure of polymers. Special techniques in analysis of macromolecules (differential enthalpymetry, inversive chromatography, optical methods). Mean molecular mass and distribution of masses - methods of measurements. Analysis of crude oil and products of petrochemistry. Sampling. Measurement of physicochemical properties, determination of base omponents (aromatic fractions, saturated, unsaturated, linear and branched hydrocarbons). GC in analysis of crude oil materials. Analysis of supplemental compounds and their classification. Important groups (fluxes, antioxidants, accelerators, antistatic agents, catalyzers, surfactants). Isolation, separation, identification and determination of surfactants in water and other ecosystems. Analysis of minerals and non-metallic materials. Decomposition and dissolution of minerals. Determination of principal components. Phase analysis. Soil analysis, determination of nutrients and organic components. Humic compounds and acids. Analysis of fertilizers. Analysis of alloys. Ferro-alloys, steels. Analysis of carbon steel grade and alloy steel. Alloys of non-ferrous metals, light and noble metals.
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Learning activities and teaching methods
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Lecture
- Attendace
- 52 hours per semester
- Homework for Teaching
- 26 hours per semester
- Preparation for the Exam
- 42 hours per semester
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Learning outcomes
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The aim is to familiarize with applications of analytical chemistry.
Define main concepts, solve typical analytical problems in the treatment of real samples of various types
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Prerequisites
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The knowledge of basics of analytical chemistry and instrumental methods of analytical chemistry is recommended.
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Assessment methods and criteria
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Mark
The student should be able to discuss the selected topics listed in Annotation (two topics).
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Recommended literature
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Beamish F.E. The Analytical Chemistry of the Noble Metals, Pergamon Press, Oxford 1966..
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Beamish F.E. The Analytical Chemistry of the Noble Metals, Pergamon Press, Oxford 1966..
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Belcher R.. Submicro Methods of Organic Analysis, Elsevier, Amsterdam 1966..
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Belcher R. Submicro Methods of Organic Analysis, Elsevier, Amsterdam 1966..
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Davídek J.:. Laboratorní příručka analýzy potravin, SNTL Praha 1985..
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Girard J.E.. Principles of Environmental Chemistry, Jones and Bartlett Publishers, Sudbury 2005..
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Girard J.E. Principles of Environmental Chemistry, Jones and Bartlett Publishers, Sudbury 2005..
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Hart F.L., Hisher H.J. Modern Food Analysis, Springer-Verlag, New York 1971..
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Hart F.L., Hisher H.J. Modern Food Analysis, Springer-Verlag, New York 1971. Wohler F., Handbookof Mineral Analysis, Henry Carey Baird, Industrial Publisher, Philadelphia 1871..
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Holzbecher Z., Churáček J. a kol. (1987). Analytická chemie. SNTL Praha.
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Mermet J.M., Otto M., Widmer H.M. Analytical Chemistry, Wiley-VCH, Weinheim 1998..
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Pearson D.. Laboratory Techniques in Food Analysis, London Butterworths, London 1973..
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Pearson D. Laboratory Techniques in Food Analysis, London Butterworths, London 1973..
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Vačková M., Smirnová L.:. Aplikovaná analytická chémia. UK Bratislava 1983..
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Wohler F. Handbookof Mineral Analysis, Henry Carey Baird, Industrial Publisher, Philadelphia 1871..
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