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Lecturer(s)
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Trach Kateryna, Mgr.
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Halman Dominik, Mgr.
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Papoušková Lucie, Mgr. Ph.D.
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Slačálek Jakub, Mgr.
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Nytka Marianna, Ph.D.
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Kučerová Pavla, RNDr. Ph.D.
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PRYSTOPIUK Oleksandr, Mgr.
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Zemek Vojtěch, Mgr.
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Součková Jitka, Mgr. Ph.D.
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Bednář Petr, doc. RNDr. Ph.D.
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Papoušková Barbora, RNDr. Ph.D.
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Skopalová Jana, doc. RNDr. Ph.D.
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Ševčík Juraj, prof. RNDr. Ph.D.
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Kurka Ondřej, RNDr. Ph.D.
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Švecová Petra, Mgr.
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Krejčí Petra, Mgr.
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Mácha Hynek, Mgr.
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Jagošová Klára, Ing.
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Nádvorníková Jana, Mgr.
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Houšť Jiří, Mgr.
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Jerga Radek, Mgr.
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Dostál Štěpán, Mgr.
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Žingor Zbyněk, Mgr.
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Pechancová Radka, RNDr. Ph.D.
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Pauk Volodymyr, Mgr. Ph.D.
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Vysloužilová Dominika, Mgr.
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Gregar Filip
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Baron Daniel, Mgr. Ph.D.
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Kučera Lukáš, doc. RNDr. Ph.D.
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Gavlová Anna, Mgr.
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Pluháček Tomáš, RNDr. Ph.D.
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Course content
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Analytical reactions of inorganic cations in characteristic groups; Selective reactions of cations; Analytical reactions of inorganic anions in characteristic groups; Selective reactions of anions; Analysis of mixtures of cations and anions; Proof of a hetero-atom in organic compounds; Basic operations and calculations in quantitative chemical analysis; Gravimetric determination of Fe3+, Ag+, Ba2+, Al3+, Ni2+, Cl-, SO42-, PO43-; Volumetric titrations: neutralization, complexometric, precipitating, redox (manganometry and iodometry); Ion exchange chromatography, Determination of the total sodium content (alkalimetry), Separation and chelatometric determination of Cu and Zn; UV/VIS spectrophotometry, Determination of Mn after oxidation using a periodate, Determination of Fe as thiocanate complex; Determination of Ni using biacetyldioxime in the presence of oxidation agent; Coulommetry and electrogravimetry (determination of Cu); Thin layer chromatography (identification of phenols in mixture). Demonstration of other instrumental techniques (AAS, IR, GC, HPLC, CE, ITP, polarography, combined techniques - HPLC/MS, GC/MS). Analysis of real samples: determination of Fe, Ca, Ni using different techniques.
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Learning activities and teaching methods
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Observation, Training in job and motor Skils
- Attendace
- 78 hours per semester
- Homework for Teaching
- 39 hours per semester
- Preparation for the Course Credit
- 33 hours per semester
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Learning outcomes
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The aim is to acquire practical skills for proof and determination of analytes.
Apply and practice fundamental analytical procedures, modify procedures for the basic analytical determinations
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Prerequisites
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The knowledge of basics of analytical chemistry is recommended.
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Assessment methods and criteria
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Written exam, Student performance
For passing the subject student has to fulfill the condition of 100% attendance in the lectures, make all the requested analytical work in correct way and elaborate suitable laboratory protocols. Student has to pass the writtent final test ( 50% of total points) as well.
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Recommended literature
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1. návody ke cvičení - dostupné u garanta cvičení..
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2. Dostál V., Šimek J., Důkaz některých anorganických iontů vybranými analytickými reakcemi, Skripta UP Olomouc 1993..
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3. Fogl J. a kol., Návody pro laboratorní cvičení z analytické chemie I., skripta VŠCHT Praha 2000.
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4. Havel J., Novotný I., Vrchlabský M. Základy analytické chemie kvantitativní. UJEP, Brno, 1981..
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5. Okáč A. Analytická chemie kvalitativní. ČSAV Praha, 1961..
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6. Churáček J., Analytická separace látek, SNTL, Praha 1990..
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7. Mermet J.M., Otto M., Widmer H.M., Analytical Chemistry, Wiley-VCH, Weinheim 1998..
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8. Instructions to particular lectures - available at guarantee of the laboratory lectures..
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