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Lecturer(s)
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Drahoš Bohuslav, doc. RNDr. Ph.D.
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Šindelář Zdeněk, doc. RNDr. CSc.
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Course content
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" general conceptions, inorganic synthesis, general features of a problem " solvents in synthesis, classification, purification methods " separation techniques in inorganig synthesis, fraction destilation, vacuum evaporation " high perssure synthesis, microwave assisted synthesis (experimental basics and principles) " hydrothermal (solvothermal) synthesis " synthesis in innert atmosphere, low temperature synthesis, reaction in liquid SO2 and NH3 resp. " intercalates " macrocyclic coordination compounds synthesis, phtallocyanines, porphyrines " complex compounds synthesis with polyazamacrocyclic ligands " transition metal complex compounds in extreme oxidation states synthesis " synthesis of transition metal complex compounds in mixed oxidation states " Schiff base in transition metal coordination compounds chemistry
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Learning activities and teaching methods
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Lecture
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Learning outcomes
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The course introduces students to the chemical processes in synthesis of inorganic and coordination compounds.
Recall basic concepts of inorganic synthesis, with a great emphasis on techniques in a chemical experiment. Describe of basic technigues in various types of inorganic synthesis (high pressure - solvatothermal synthesis, innert atmosphere, microwave assisted, extremal temperature etc.) and other synthetic methods used in coordination chemistry.
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Prerequisites
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For the successful completion of the colloquium, the student must achieve at least a 70% success rate in the written test.
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Assessment methods and criteria
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Written exam
50% successfulness in written test (sayllabus extent).
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Recommended literature
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(2013). Comprehensive Inorganic Chemistry II, 2nd ed., vybrané kapitoly.
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Inorganic synthesis.
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původní literatura.
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G. Brauer a kol. (1975). Handbuch der Präparativen Anorganischen Chemie (existuje šestidílný ruský překlad dostupný v SVK Olomouc sgn. 535787). Verlag, Stuttgart.
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J. Gaľecki. (1964). Preparatyka nieorganiczna. NT, Warszawa.
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N. N. Čarnajev ed. (1964). Sintěz komplexnych soediněnij metallov platinovoj grupy. Nauka, Moskva.
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