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Lecturer(s)
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Milde David, doc. Ing. Ph.D.
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Course content
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Quality of chemical analysis results and its security. Metrology in chemistry - reference materials, metrological traceability. Laboratory accreditation. Internal and external quality assurance (control charts, interlaboratory comparison of tests). Validation of methods. Measurement uncertainty. Fundamentals of sampling.The seminar includes an introduction to theoretical fundamentals and practical exercises
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Learning activities and teaching methods
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Dialogic Lecture (Discussion, Dialog, Brainstorming)
- Attendace
- 26 hours per semester
- Homework for Teaching
- 13 hours per semester
- Preparation for the Course Credit
- 21 hours per semester
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Learning outcomes
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The aim is to acquaint with basics of metrology in chemistry.
Manage proper operation of the analytical laboratory, propose proper operational procedures
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Prerequisites
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The knowledge of basics of general, organic, anorganic, physical, analytical chemistry and biochemistry is recommended.
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Assessment methods and criteria
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Written exam, Student performance
50% success in a written test and the ability to discuss the selected theme of the subject
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Recommended literature
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Suchánek M.: Kvalimetrie 7. Validaceanalytických metod. Eurachem ČR, Praha 1997..
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Suchánek M.:Kvalimetrie 14. Návaznost chemických měření, Používání referenčních materiálů v chemické analýze. Eurachem ČR, Praha2004..
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Krejčová A. Zabezpečení jakosti výsledků analýz v chemické laboratoři. Univerzita Padrubice, Pardubice 2010.
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Prichard E., Bawick V. Quality Assurance in Analytical Chemistry, Wiley, Weinheim 2007.
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S.L.R. Ellison, V. Barwick, T.J.D. Farrant. (2009). Practical Statistic for Analytical Scientist, A Bench Guide, 2nd Ed. RSC. Cambridge.
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Suchánek M., Milde D. (2015). Kvalimetrie 20: Vhodnost analytických metod pro daný účel. Praha.
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Suchánek M. 17. mezilaboratorní porovnání a zkošení způsobilosti. Eurachem ČR, Praha 2010.
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Wenclawiak B.W., Koch M., Hadjicostas E. Quality Assurance in Analytical Chemistry. Springer Verlag, Berlin 2010.
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